Mokhoa oa tlhahiso le tšebeliso ea N-ethyl-N-cyanoethylaniline

Mokhoa oa tlhahiso:

Sebelisa AlC13 e sa haellang e le sesebelisoa sa ho susumetsa karabelo pakeng tsa N-ethylaniline le acrylonitrile. Maemo a ntlafalitsoeng ke: eketsa 10% ea boima ba N-ethylaniline e sa haellang AlC13, u arabele mochesong o ka bang 80°C ka lihora tse 6-8, 'me sekhahla sa phetoho se fihla ho 98.5%, ka chai e fetang 97%.
Mokhoa o mong o sebelisa N-ethylaniline le chloroethanol tlas'a catalysis ea metheo e sa tloaelehang kapa letsoai ho e kopanya mochesong oa 120-130°C. Poelo e ka fihla ho 90%, empa metsi a litšila a thehoa ts'ebetsong.
sebelisa:

E sebelisoa haholo-holo e le thepa e tala ea mantlha bakeng sa 'mala o mosehla o sootho o hasaneng, lamunu e hasaneng le lidae tse ling.
E boetse e sebelisoa masimong a lik'hemik'hale tse kang metsoako ea meriana, metsoako ea chefo e bolaeang likokoanyana, metsoako ea amino, metsoako ea nitrile, jj.

N-ethyl-N-cyanoethylaniline e sebelisoa haholo-holo e le karolo ea dae. Tlhoko ea eona ea 'maraka e bonahala haholo indastering ea dae, moo e sebelisetsoang ho hlahisa sootho bo mosehla bo hasaneng, lamunu e hasaneng le lidae tse ling tse hasaneng.
Ho phaella moo, N-ethyl-N-cyanoethylaniline e boetse e sebediswa masimong a dikhemikhale a kang di-intermediate tsa meriana, di-intermediate tsa dibolayadikokwanyana, di-amino compounds, le di-nitrile compounds. Tlhokeho masimong ana le yona ke karolo ya mmaraka wa yona.

Ka bokhutšoanyane, tlhoko ea 'maraka ea N-ethyl-N-cyanoethylaniline e shebane haholo le indasteri ea dae le liindasteri tse ling tsa lik'hemik'hale, 'me e bapala karolo ea bohlokoa e le thepa ea bohlokoa e tala liindastering tsena.

Thepa ea Lik'hemik'hale ea 3-Ethylanilinopropiononitrile
Boemo ba ho belisa 137-140°C 4mm
bongata ba 1,03 g/cm3
index ea refractive 1.6210 (khakanyo)
pka 5.27±0.50 (E boletsoeng esale pele)
etsa mokelikeli o hlakileng
'Mala o se nang 'mala ho isa ho o mosehla
Matla a khoheli a itseng 1.03
Referense ea CAS Database 148-87-8 (Referense ea CAS Database)
NIST Khemistri Referense Propionitrile, 3-(n-ethylanilino)-(148-87-8)
Sistimi ea Ngoliso ea Lintho tsa EPA Propanenitrile, 3-(ethylphenylamino)- (148-87-8)

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