CAS:118753-70-1丨N-Boc-N,N-Bis(2-Chloroethyl)Amine
N,N-bis(2-chloroethyl)carbamate tert-butyl ester e ka sebediswa e le mokediketsi wa k'hemistri ya meriana le tlhahiso ya organic. Diphetohong tsa tlhahiso ya organic, sehlopha sa Boc sebopehong se ka tloswa habonolo ho fumana sehlopha se sebetsang sa carboxyl.
Mokhoa oa maiketsetso o kenyelletsa ho hlohlelletsa ka potlako ho emisoa ha bis-(2-chloroethyl)amine hydrochloride (5 g, 0.028 mol) ka har'a dichloromethane (42 mL) ka1Tharollo ea metsi ea 0% sodium hydroxide (28 mL) mochesong oa ho hlapa ka leqhoa. Tharollo ea di-tert-butyl dicarbonate (6.11 g, 0.028 mol) ka har'a dichloromethane (28 mChemicalbook L) e eketsoa. Kamora ho hlohlelletsa mochesong oa kamore ka lihora tse 18.5, dichloromethane (30 mL) e eketsoa butle-butle motswakong oa karabelo. Mekhahlelo e 'meli e aroloa. Mokhahlelo oa metsi o ntšoa hape ka dichloromethane (30 mL). Mekhahlelo e kopaneng ea lintho tse phelang e omisoa holim'a anhydrous magnesium sulfate, e sefshoe, 'me e kopantsoe ho fumana N,N-bis(2-chloroethyl)carbamate tert-butyl.














